Publications by authors named "Alessia Ciogli"

58Publications

Synthesis of pyrano[2,3-f]chromen-2-ones vs. pyrano[3,2-g]chromen-2-ones through site controlled gold-catalyzed annulations.

Org Biomol Chem 2019 12;17(47):10065-10072

Dipartimento di Scienze Fisiche e Chimiche Università degli Studi di L'Aquila, Via Vetoio, 67100 Coppito (AQ), Italy.

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http://dx.doi.org/10.1039/c9ob01695cDOI Listing
December 2019

Modular and conservative procedure for the quantification of amino functionalities bonded to solid porous matrices.

Anal Chim Acta 2019 Aug 9;1068:120-130. Epub 2019 Apr 9.

Dipartimento di Chimica e Tecnologie del Farmaco, Università degli Studi di Roma "La Sapienza", Piazzale Aldo Moro 5, 00185, Roma, Italy. Electronic address:

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http://dx.doi.org/10.1016/j.aca.2019.04.006DOI Listing
August 2019

Direct analysis of chiral active pharmaceutical ingredients and their counterions by ultra high performance liquid chromatography with macrocyclic glycopeptide-based chiral stationary phases.

J Chromatogr A 2018 Nov 17;1576:42-50. Epub 2018 Sep 17.

Dipartimento di Chimica e Tecnologie del Farmaco, "Sapienza" Università di Roma, P. le Aldo Moro 5, 00185 Roma, Italy. Electronic address:

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http://dx.doi.org/10.1016/j.chroma.2018.09.029DOI Listing
November 2018

Aggregation behaviour of triphenylphosphonium bolaamphiphiles.

J Colloid Interface Sci 2018 Dec 18;531:451-462. Epub 2018 Jul 18.

CNR-IMC-Sezione Meccanismi di Reazione-UOS di Roma c/o Department of Chemistry, Sapienza University, P.le A. Moro 5, Roma, Italy. Electronic address:

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http://dx.doi.org/10.1016/j.jcis.2018.07.067DOI Listing
December 2018

Synthesis of Bromoundecyl Resorc[4]arenes and Applications of the Cone Stereoisomer as Selector for Liquid Chromatography.

J Org Chem 2018 08 11;83(15):7683-7693. Epub 2018 Jun 11.

Dipartimento di Chimica e Tecnologie del Farmaco , Sapienza Università di Roma , P.le A. Moro 5 , 00185 Roma , Italy.

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http://dx.doi.org/10.1021/acs.joc.8b00488DOI Listing
August 2018

Recognition mechanism of aromatic derivatives resolved by argentation chromatography: The driving role played by substituent groups.

Anal Chim Acta 2018 Aug 20;1019:135-141. Epub 2018 Feb 20.

Department of Chemistry and Technology of Drug, Sapienza University of Rome, P. le Aldo Moro 5, 00185, Rome, Italy. Electronic address:

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http://dx.doi.org/10.1016/j.aca.2018.02.038DOI Listing
August 2018

Enantioselective ultra high performance liquid and supercritical fluid chromatography: The race to the shortest chromatogram.

J Sep Sci 2018 Mar 2;41(6):1307-1318. Epub 2018 Feb 2.

Dipartimento di Chimica e Tecnologie del Farmaco, "Sapienza" Università di Roma, Rome, Italy.

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http://dx.doi.org/10.1002/jssc.201701406DOI Listing
March 2018

Future perspectives in high efficient and ultrafast chiral liquid chromatography through zwitterionic teicoplanin-based 2-μm superficially porous particles.

J Chromatogr A 2017 Oct 6;1520:91-102. Epub 2017 Sep 6.

Dipartimento di Chimica e Tecnologie del Farmaco, "Sapienza" Università di Roma, P. le Aldo Moro 5, 00185 Roma, Italy. Electronic address:

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http://dx.doi.org/10.1016/j.chroma.2017.09.008DOI Listing
October 2017

Experimental evidence of the kinetic performance achievable with columns packed with new 1.9μm fully porous particles of narrow particle size distribution.

J Chromatogr A 2016 Jul 12;1454:86-92. Epub 2016 May 12.

Applied Research and Development, Millipore Sigma, 595 North Harrison Road, Bellefonte, PA 16823, USA.

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http://dx.doi.org/10.1016/j.chroma.2016.05.038DOI Listing
July 2016

Ultra-fast high-efficiency enantioseparations by means of a teicoplanin-based chiral stationary phase made on sub-2 μm totally porous silica particles of narrow size distribution.

J Chromatogr A 2016 Jan 2;1427:55-68. Epub 2015 Dec 2.

Dipartimento di Chimica e Tecnologie del Farmaco, Sapienza Università di Roma, P.le Aldo Moro 5, 00185 Roma, Italy. Electronic address:

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http://dx.doi.org/10.1016/j.chroma.2015.11.071DOI Listing
January 2016

Stereolability of chiral ruthenium catalysts with frozen NHC ligand conformations investigated by dynamic-HPLC.

Chirality 2015 Oct 6;27(10):685-92. Epub 2015 Aug 6.

Department of Chemistry and Technology of Drug, "Sapienza" University of Rome, Rome, Italy.

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http://dx.doi.org/10.1002/chir.22487DOI Listing
October 2015

Organocatalytic atroposelective formal Diels-Alder desymmetrization of N-arylmaleimides.

Org Lett 2015 Apr 17;17(7):1728-31. Epub 2015 Mar 17.

†Department of Industrial Chemistry "Toso Montanari", Alma Mater Studiorum-University of Bologna, Viale del Risorgimento 4, 40136 Bologna, Italy.

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http://dx.doi.org/10.1021/acs.orglett.5b00509DOI Listing
April 2015

Expanding the potential of chiral chromatography for high-throughput screening of large compound libraries by means of sub-2μm Whelk-O 1 stationary phase in supercritical fluid conditions.

J Chromatogr A 2015 Feb 22;1383:160-8. Epub 2015 Jan 22.

Dipartimento di Chimica e Tecnologie del Farmaco, "Sapienza" Università di Roma, P.le Aldo Moro 5, 00185 Roma, Italy. Electronic address:

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http://dx.doi.org/10.1016/j.chroma.2015.01.042DOI Listing
February 2015

Dynamic high performance liquid chromatography on chiral stationary phases. Low temperature separation of the interconverting enantiomers of diazepam, flunitrazepam, prazepam and tetrazepam.

J Chromatogr A 2014 Oct 12;1363:144-9. Epub 2014 Aug 12.

Sapienza Università di Roma. Dipartimento di Chimica e Tecnologie del Farmaco, P.le A. Moro 5, 00185 Rome, Italy. Electronic address:

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http://dx.doi.org/10.1016/j.chroma.2014.07.097DOI Listing
October 2014

Toward enantioselective nano ultrahigh-performance liquid chromatography with Whelk-O1 chiral stationary phase.

Electrophoresis 2014 Oct 14;35(19):2819-23. Epub 2014 Aug 14.

Department of Drug Chemistry and Technology, "Sapienza" University of Rome, Rome, Italy.

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http://dx.doi.org/10.1002/elps.201400240DOI Listing
October 2014

Remote control of axial chirality: aminocatalytic desymmetrization of N-arylmaleimides via vinylogous Michael addition.

J Am Chem Soc 2014 Jul 11;136(29):10250-3. Epub 2014 Jul 11.

Department of Industrial Chemistry "Toso Montanari", Alma Mater Studiorum-University of Bologna , Viale del Risorgimento 4, 40136-Bologna- Italy.

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http://dx.doi.org/10.1021/ja505610kDOI Listing
July 2014

ABCB1 Structural Models, Molecular Docking, and Synthesis of New Oxadiazolothiazin-3-one Inhibitors.

ACS Med Chem Lett 2013 Aug 13;4(8):694-8. Epub 2013 May 13.

Dip. di Chimica "G. Ciamician", Università degli Studi di Bologna , Via F. Selmi 2, 40126 Bologna, Italy.

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http://dx.doi.org/10.1021/ml300436xDOI Listing
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC4027559PMC
August 2013

Understanding mixed-mode retention mechanisms in liquid chromatography with hydrophobic stationary phases.

Anal Chem 2014 May 28;86(10):4919-26. Epub 2014 Apr 28.

Department of Chemistry and Pharmaceutical Sciences, University of Ferrara , via L. Borsari, 46, 44121 Ferrara, Italy.

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http://dx.doi.org/10.1021/ac500248bDOI Listing
May 2014

The experimental observation of the intramolecular NO₂/CO interaction in solution.

Angew Chem Int Ed Engl 2014 May 9;53(21):5405-9. Epub 2014 Apr 9.

Department of Industrial Chemistry "Toso Montanari", Alma Mater Studiorum-University of Bologna, Viale Risorgimento 4, 40136 Bologna (Italy) http://www2.fci.unibo.it/∼mazzand.

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http://dx.doi.org/10.1002/anie.201402366DOI Listing
May 2014

Separation of complex sugar mixtures on a hydrolytically stable bidentate urea-type stationary phase for hydrophilic interaction near ultra high performance liquid chromatography.

J Sep Sci 2014 Mar 25;37(5):527-35. Epub 2014 Jan 25.

Dipartimento di Chimica e Tecnologie del Farmaco, Sapienza Università di Roma, Roma, Italy.

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http://dx.doi.org/10.1002/jssc.201301008DOI Listing
March 2014

Chiral supramolecular selectors for enantiomer differentiation in liquid chromatography.

Top Curr Chem 2013 ;340:73-105

Dipartimento di Chimica e Tecnologie del Farmaco, Sapienza Università di Roma, P.le Aldo Moro 5, 00185, Rome, Italy.

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http://link.springer.com/content/pdf/10.1007/128_2013_452.pd
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http://link.springer.com/10.1007/128_2013_452
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http://dx.doi.org/10.1007/128_2013_452DOI Listing
May 2014

Atropisomers of arylmaleimides: stereodynamics and absolute configuration.

J Org Chem 2013 Apr 8;78(8):3709-19. Epub 2013 Apr 8.

Department of Industrial Chemistry Toso Montanari, University of Bologna, Viale Risorgimento 4, 40136-Bologna, Italy.

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http://dx.doi.org/10.1021/jo400200vDOI Listing
April 2013

A new method to investigate the intrusion of water into porous hydrophobic structures under dynamic conditions.

Anal Chem 2013 Jan 13;85(1):19-22. Epub 2012 Dec 13.

Department of Chemistry and Pharmaceutical Sciences, University of Ferrara , Italy.

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http://dx.doi.org/10.1021/ac303253bDOI Listing
January 2013

Enantioselective ultra-high and high performance liquid chromatography: a comparative study of columns based on the Whelk-O1 selector.

J Chromatogr A 2012 Dec 19;1269:226-41. Epub 2012 Sep 19.

Dipartimento di Chimica e Tecnologie del Farmaco, Sapienza Università di Roma, P.le Aldo Moro 5, 00185 Roma, Italy.

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http://dx.doi.org/10.1016/j.chroma.2012.09.035DOI Listing
December 2012

Introducing enantioselective ultrahigh-pressure liquid chromatography (eUHPLC): theoretical inspections and ultrafast separations on a new sub-2-μm Whelk-O1 stationary phase.

Anal Chem 2012 Aug 9;84(15):6805-13. Epub 2012 Jul 9.

Dipartimento di Chimica e Tecnologie del Farmaco, Sapienza Università di Roma, P. le Aldo Moro 5, 00185 Roma, Italy.

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http://dx.doi.org/10.1021/ac301335bDOI Listing
August 2012

Design and evaluation of hydrolytically stable bidentate urea-type stationary phases for hydrophilic interaction chromatography.

J Chromatogr A 2012 Apr 14;1232:196-211. Epub 2011 Dec 14.

Dipartimento di Chimica e Tecnologie del Farmaco, Sapienza Università di Roma, P.le Aldo Moro 5, 00185 Roma, Italy.

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http://dx.doi.org/10.1016/j.chroma.2011.12.028DOI Listing
April 2012

New anthranilic acid based antagonists with high affinity and selectivity for the human cholecystokinin receptor 1 (hCCK1-R).

J Med Chem 2011 Aug 20;54(16):5769-85. Epub 2011 Jul 20.

Department of Chemical and Pharmaceutical Sciences, University of Trieste, P.le Europa 1, 34127 Trieste, Italy.

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http://dx.doi.org/10.1021/jm200438bDOI Listing
August 2011

Hybrid polyacrylamide chiral stationary phases for HPLC prepared by surface-initiated photopolymerization.

J Sep Sci 2010 Oct;33(19):3022-32

Dipartimento di Chimica e Tecnologie del Farmaco, Sapienza Università di Roma, Roma, Italy.

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http://dx.doi.org/10.1002/jssc.201000355DOI Listing
October 2010

An unexpected highly stereoselective bisaziridination of (E,E)-1,4-dialkyl-2,3-dinitrobutadienes followed by a nitro group driven ring enlargement.

J Org Chem 2009 Dec;74(24):9314-8

Dipartimento di Chimica e Tecnologie del Farmaco, Università degli Studi La Sapienza, Piazzale A. Moro 5, I-00185 Roma, Italy.

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http://dx.doi.org/10.1021/jo902112jDOI Listing
December 2009

Binding of dipeptides and amino acids to Teicoplanin chiral stationary phase: apparent homogeneity of some heterogeneous systems.

Anal Chem 2009 Aug;81(16):6735-43

Department of Chemistry, University of Ferrara, via L. Borsari 46, I-44100 Ferrara, Italy.

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http://dx.doi.org/10.1021/ac900677fDOI Listing
August 2009

Dynamic HPLC of stereolabile iron(II) complexes on chiral stationary phases.

Chirality 2009 Jan;21(1):97-103

Dipartimento di Studi di Chimica e Tecnologia delle Sostanze Biologicamente Attive, Università di Roma La Sapienza, 00185 Roma, Italy.

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http://dx.doi.org/10.1002/chir.20612DOI Listing
January 2009

Enantiomerization of chiral uranyl-salophen complexes via unprecedented ligand hemilability: toward configurationally stable derivatives.

J Org Chem 2008 Aug 16;73(16):6108-18. Epub 2008 Jul 16.

Dipartimento di Studi di Chimica e Tecnologia delle Sostanze Biologicamente Attive, Universita La Sapienza, Piazzale Aldo Moro 5, 00185 Roma, Italy.

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http://dx.doi.org/10.1021/jo800610fDOI Listing
August 2008

On-column epimerization of dihydroartemisinin: an effective analytical approach to overcome the shortcomings of the International Pharmacopoeia monograph.

J Chromatogr B Analyt Technol Biomed Life Sci 2008 Nov;875(1):180-91

Analytical Development, R&D Department, sigma-tau S.p.A., Via Pontina km 30,400, 00040 Pomezia, Italy.

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http://dx.doi.org/10.1016/j.jchromb.2008.06.037DOI Listing
November 2008

Efficient Thia-bridged triarylamine heterohelicenes: synthesis, resolution, and absolute configuration determination.

Chemistry 2008 ;14(19):5747-50

Dipartimento di Chimica Organica e Laboratorio di Progettazione e Sintesi di Eterocicli Biologicamente Attivi (HeteroBioLab), Università di Firenze, Via della Lastruccia 13, 50019 Sesto Fiorentino, Firenze (Italy).

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http://dx.doi.org/10.1002/chem.200800705DOI Listing
September 2008

New chiral and restricted-access materials containing glycopeptides as selectors for the high-performance liquid chromatographic determination of chiral drugs in biological matrices.

J Chromatogr A 2008 May 3;1191(1-2):205-13. Epub 2007 Dec 3.

Dipartimento di Studi di Chimica e Tecnologia delle Sostanze Biologicamente Attive, Università La Sapienza, P.le Aldo Moro 5, 00185 Rome, Italy.

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http://dx.doi.org/10.1016/j.chroma.2007.11.098DOI Listing
May 2008

Synthesis and characterization of novel internal surface reversed-phase silica supports for high-performance liquid chromatography.

J Chromatogr A 2007 Dec 25;1176(1-2):79-88. Epub 2007 Oct 25.

Dipartimento di Studi di Chimica e Tecnologia delle Sostanze Biologicamente Attive, Università La Sapienza, P.le Aldo Moro 5, 00185 Rome, Italy.

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http://dx.doi.org/10.1016/j.chroma.2007.10.062DOI Listing
December 2007

A general procedure for the synthesis of stereochemically pure conduritol derivatives practical also for solid-phase chemistry.

J Comb Chem 2006 Jan-Feb;8(1):74-8

Dipartimento di Chimica Organica "A. Mangini", University of Bologna, Viale Risorgimento 4, I-40136 Bologna, Italy. cere@ ms.fci.unibo.it

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http://dx.doi.org/10.1021/cc050053iDOI Listing
February 2006

Study of mechanisms of chiral discrimination of amino acids and their derivatives on a teicoplanin-based chiral stationary phase.

J Chromatogr A 2004 Mar;1031(1-2):143-58

Department of Chemistry, University of Ferrara, Via L. Borsari 46, Ferrara I-44100, Italy.

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http://dx.doi.org/10.1016/j.chroma.2003.10.090DOI Listing
March 2004